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Photoelectron spectroscopy (PES) is the energy measurements of photoelectrons emitted from solids, gases, or liquids by the photoelectric effect. Photoelectron spectroscopy is an extension of the photoelectric effect – Einstein's famous experiment, which allowed him to observe the emission ofPhotoelectron spectroscopy uses monochromatic sources of radiation (i.e. photons of fixed energy). Page 5. In XPS the photon is absorbed by an atom in a Photoelectron Spectroscopy: General Principle. Surface sensitivity. Instrumentation. Background subtraction. PES peaks, loss features. Peak fitting. Photoelectron Spectroscopy: Principles And Applications [PDF] [15mbrm1ioshg]. Photoelectron Spectroscopy presents an up-to-date introduction to the field by X-ray Photoelectron Spectroscopy (XPS), also known as Electron Spectroscopy for Chem.ical Analysis (ESCA), is wide- ly used LO investigate the chemical Photoelectron spectroscopy (PES) is the energy measurements of photoelectrons emitted from solids, gases, or liquids by the photoelectric effect. Depending on this monograph is called photoelectron spectroscopy (if one wants to name it by the particle that is being detected) or photoemission spectroscopy (if one.